Alumina: discriminative analysis using 3D correlation of solid-state NMR parameters
نویسندگان
چکیده
منابع مشابه
ucture using solid-state NMR
An overview of solid-state NMR structural studies on various silk forms and analogs conducted by the authors' research groups is presented. The well-studied silkworm and spider silks together with related silk peptides have a mixture of secondary structures including b-sheet, b-turn, helix and random coil that are difficult to analyze by X-ray diffraction and electron microscopy but convenientl...
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0009-2614/$ see front matter 2012 Elsevier B.V. A http://dx.doi.org/10.1016/j.cplett.2012.05.030 q First presented at the 53rd Rocky Mountain Con istry, August 2010, Snowmass, Colorado, USA. ⇑ Corresponding author at: Ecole Normale Supérie 24 rue Lhomond, 75231 Paris cedex 05, France. E-mail address: [email protected] (P. Tekely). The intrinsic asymmetry of 2D solid-state homonuclear NMR corr...
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Perdeuteration of biological macromolecules for magic angle spinning solid-state NMR spectroscopy can yield high-resolution (2)H-(13)C correlation spectra and the method is therefore of great interest for the structural biology community. Here we demonstrate that the combination of sample deuteration and dynamic nuclear polarization yields resolved (2)H-(13)C correlation spectra with a signal e...
متن کاملSolid-State NMR Spectroscopy
A number of arylamides have been synthesized and found to exhibit potent antimicrobial activities against a broad spectrum of Gram-positive and Gram-negative bacteria while exhibiting low toxicity toward eukaryotic cells. These facially amphiphilic foldamers have a relatively rigid intramolecular hydrogen-bonded arylamide as a framework, which places trifluormethyl versus positively charged ami...
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The past decade has seen significant advances in the technique of nuclear magnetic resonance as applied to condensed phase systems. This progress has been driven by the development of sophisticated radio-frequency pulse sequences to manipulate nuclear spins, and by the availability of high-field spectrometers. During this period it has become possible to predict the major NMR observables using ...
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ژورنال
عنوان ژورنال: Chemical Society Reviews
سال: 2019
ISSN: 0306-0012,1460-4744
DOI: 10.1039/c8cs00321a